Chromatographiebedarf

Schaltventile, Mitteldruckventile, Shut-off Ventile, Split Ventile, Purge Ventile

ELECTRONIC ACTUATORS
- With Factory Premounted Valve / Safety Tested and Rated to Conform to ETL, CSA  Specifications
All of our valves  are available premounted on compact Electronic Actuators to automate valve positioning. Our valves are coupled with a DC gear motor, which offers outstanding rotational accuracy and low actuation times.
Upchurch Scientific actuated valves can be conveniently operated by keypad or computer controlled through contact closure and RS-232 communication. LED indicators on the actuator keypad specify valve position. Additionally, valves may be multiplexed (daisy-chained) for custom automation solutions when using RS-232 communication

Schaltventile

DC Gear Motor Actuated Valves

Each actuator is provided with an inline power adapter which allows operation from both 110/1 20V (North American) and 220/240V (European) AC power. All actuators come with a one-year parts and labor warranty.

 

VALVES INTRODUCTION
-
Injection and Selection Valves for Pressures to 1,000 psi (69 bar) / Switching and Shut-Off Valves for Pressures to 500 psi (34 bar) / Directly Connect 1/16" or 1/8" OD Tubing with Fangeless Fittings / Manual and Actuated Versions

 

Uphurch Scientific® Medium Pressure Valves are available for 1/16" or 1/8" OD tubing in sample injection or six-way flow selection versions. These valves have completely biocompatible flow paths and are perfect for systems where the pressure does not exceed 500 - 1,000 psi (34 - 69 bar), including flow injection analysis (FIA) and some chromatography applications. These valves come in manual (with or without a bulkhead mounting option) and electronically actuated versions.

The Medium Pressure Valve series also includes our Switching Valves (rated to500 psi, 34 bar) which offer several options for directional flow control. The most popular is the "L" style - a two-way switching valve that could be used for mobile phase, column or detector selection between two inlets or outlets. Use the "T" style valve with a plug to change a three-way open connection to a two-way selection valve. The "D" style valve is a two position four-way switching valve where adjacent ports are connected by a flow path which rotates 90° to change position. Applications for this valve include protection of column or other sensitive instrument components during a cleaning cycle. These biocompatible four-port switching valves are available for manual control or mounted onto an electronic actuator. Polymer inline shut-off valves are also available for 1/8" or 1/16" OD tubing to quickly turn a flow stream "on" or "off".

 

Micro-Metering and Micro-Splitter Needle Valves
- Fine Control of Flow in Two-way or Three-way Valves
/ Applicable to a Wide Range of Applications, including Interfacing LC/MS Systems / Ability to Reduce 1ml/min Incoming Flow Rate to as Low as 2µL/min! / Versions for Capillary up to 1/8" OD Tubing

Upchurch Scientific Needle Valves control flow of either the output of a two-port valve (Micro-Metering) or on the split stream of a three-port valve (MicroSplitter Valves). Use one of these valves to regulate gas flow in a helium sparging system or to split post-column flow to a mass spectrometer. Several versions are available for connecting different tubing sizes, and biocompatible equivalents of each are offered.

 

Prime/Purge Valves
Upchurch Scientific also offers two styles of pump Prime/Purge Valves, one for use with Waters® HPLC instruments and a universal low pressure version. Both feature easy, luer-actuated operation.

 

MEDIUM PRESSURE INJECTION VALVES
- Biocompatible and Inert / Low Swept Volume / Minimal Dispersion

Upchurch Scientific® 6-Port Medium Pressure Injection Valves feature easy, external sample loop customization. Simply clean-cut a piece of tubing that represents the volume of sample you wish to inject, taking into account the port-to-port volume of the valve.
Two biocompatible injection valve options are available:

Long-Life Ceramic


Featuring ceramic-to-ceramic sealing surfaces, these new long-life valves have been tested to over one million actuations with no change in performance (1). The wetted materials are chemically resistant ceramic and PEEK™ polymer and the valves are rated to 500 psi (34 bar). Each valve includes 1/4-28 Flangeless Fittings for 1/16" OD tubing.

VIEWPOINT FROM ROTARY KNOB

Flow path of Medium Pressure Injection Valvesb   (highlighting flow through sample loop in each position)

Economical Polymer

These economical valves have chemically resistant Vespel® and Teflon® wetted surfaces and are rated for a maximum pressure of 1,000 psi (69 bar). Each valve includes 1/4-28 Flangeless Fittings for 1/16" or 1/8" OD tubing.
Both valve options are available in three configurations: standard manual, bulkhead mountable manual, and actuated.

(1) Tested using room-temperature water as the solvent.

 

MANUAL VALVE DIMENSION (EXCLUDING FITTINGS)
Valve Typ Sealing Surface Dimension (L x W)
Standard Polymer
2.72" x 1.24"(1)
(69.1 x 31.5 mm)
Ceramic
2.75" x 1.30" (69.8 x 33.0 mm)
Bulkhead Mountable Polymer
2.92" x 1.24"(1) (74.2 x 31.5 mm)
Ceramic
3.00" x 1.30" (76.2 x 33.0 mm)
(1) Width of the knob, which is slightly wider than the valve body.

 

MEDIUM PRESSURE INJECTION PORT ADAPTER
Our simple, biocompatible adapter converts any 1/4-28 flat-bottom port into a port that can accept a standard 22 gauge HPLC injection needle. This injection port adapter is adjustable, so you can create a snug fit around the needle to prevent any leaking of the analyte. In addition, this product features an internal stop that prevents you from inserting the needle too far, eliminating the possibility of damaging the valve with the needle tip.

 

Artikelnummer Beschreibung Preis in €
MEDIUM PRESSURE INJECTION VALVES, MANUAL
M-460 Injection Valve (1), Ceramic, for 1/16" OD tubing .040" thru-hole, 16.9µl swept volume (2), Black 533,23
M-461 Bulkhead version of M-460 (1) 558,67
V-450 Injection Valve (1), Polymer, for 1/16" OD tubing .040" thru-hole, 5.1 µl swept volume', Black 217,12
V-451 Bulkhead version of V-450 (1) 225,67
V-540 Injection Valve (3), Polymer, for 1/8" OD tubing .063" thru-hole, 12.7µl swept volume (3), Red 283,97
V-541 Bulkhead version of V-540 (3) 295,10
V-104 5/64" Allen Wrench (replacement) 2,50
MEDIUM PRESSURE INJECTION VALVES, ACTUATED
V-1451-DC Actuated version of V-451, DC Gear (premounted)(4) 1574,15
V-1541-DC Actuated version of V-541, DC Gear (premounted)(4) 1574,15
V-1461-DC Actuated version of M-461, DC Gear (premounted)(4) 2723,11
MEDIUM PRESSURE INJECTION PORT ADAPTER
P-295 Adjustable Injection Port Adapter 13,18
P-296 Replacement Tubing/Ferrule Assembly 6,59
(1) Comes complete with P-235/P-200 Flangeless Fittings
(2) Per pathway. Three pathways per valve (3)
(3) Comes complete with P-335/P-340 Flangeless Fittings
(4) Actuated valves also include: (1) serial port adapter; (1) each RS-232 and contact closure
communications cables (1) power adapter (1) each North American style and European style power
cord DC gear actuated valves come with a communication cable for multiplex (daisy-chain) operations.

 

MEDIUM PRESSURE 6-WAY SELECTION VALVES
- Biocompatible and Inert
/ Low Swept Volume / Excellent Choice for Mobile Phase Selection
Patented Upchurch Scientific® 6-Way Medium Pressure Selection Valves have a common inlet (or outlet) port connected to six different ports. Use these valves to select between multiple solvent reservoirs without having to disconnect and reconnect lines. Or, use two valves in conjunction with each other to serve as a column selection system in a moderate pressure semi-prep or high-flow analytical application. Two biocompatible selection valve options are available:

Long-Life Ceramic

Featuring ceramic-to-ceramic sealing surfaces, these new long-life valves have been tested to over one million actuations with no change in performance.(1) The wetted materials are chemically resistant ceramic and PEEK" polymer and the valves are rated to 500 psi (34 bar). Each valve includes 1/4-28 Flangeless Fittings for 1/16" OD tubing.

(1) Tested using room-temperature water as the solvent

Mitteldruck Schaltventile bis 34 bar

Economical Polymer

These economical valves have chemically resistant Vespel® and Teflon® wetted surfaces and are rated for a maximum pressure of 1,000 psi (69 bar). Each valve includes 1/4-28 Flangeless Fittings for 1/16" or 1/8" OD tubing.
If your application does not require all six outer ports, seal the extra port(s) with any flat-bottom 1/4-28 plug.Both valve options are available in three configurations: standard manual, bulkhead mountable manual, and actuated.  Dimensions of the manual selection valves are the same as that of the injection valves.

Artikelnummer Beschreibung Preis in €
MEDIUM PRESSURE 6-WAY SELECTION VALVES, MANUAL
M-470 6-Way Selection Valve(1), Ceramic for 1/16" OD tubing ,040" thru-hole, 16.1 µl swept volume, Black 578,24
M-471 Bulkhead version of M-471 (1) 588,65
V-240 6-Way Selection Valve(1), Polymer, for 1/16" OD tubing .040" thru-hole, 11,5 µl swept volume, Black 199,00
V-241 Bulkhead version of V-240 (1) 209,81
V-340 6-Way Selection VaIve(2), Polymer, for 1/8" OD tubing .063" thru-hole, 18.1 µl swept volume, Red 218,98
V-341 Bulkhead version of V-340 (2) 226,50
V-104 5/64" Allen Wrench (replacement) 2,50
MEDIUM PRESSURE 6-WAY SELECTION VALVES, ACTUATED
V-1241-DC Actuated version of V-241, DC Gear (premounted) (3) 1574,15
V-1341-DC Actuated version of V-341, DC Gear (premounted) (3) 1574,15
V-1471-DC Actuated version of V-471, DC Gear (premounted) (3) 2723,11
(1) Comes complete with P-235/P-200 Flangeless Fittings
(2) Comes complete with P-335/P-340 Flangeless Fittings.
(3) Actuated valves also include: (1) serial port adapter (1) each RS-232 and contact closure communications cables; (1) power adapter; (1) each North American style and European style power cord. DC gear actuated valves come with a communication cable for multiplex (daisy-chain) operations.

 

MEDIUM PRESSURE 4-PORT SWITCHING VALVES
- Three Configurations to Choose From / Biocompatible Flow Paths
Mitteldruck 4 Kanal Schaltventil With three versions to choose from, Upchurch Scientific® Switching Valves offer many flow distribution combinations. Each valve has a low swept volume, can withstand pressures to 500 psi (34 bar), is chemically inert and biocompatible. The PEEKTM and TeflonTM construction results in a valve as durable as it is economical. Each V-100 Series Switching Valve has .040" thru-holes and is supplied with Flangeless Fittings for use with 1/16" OD tubing. To use these valves with 1/8" OD tubing, simply replace the supplied fittings with 1/4-28 Flangeless Fittings. You may notice a slight back pressure at higher flow rates, due to the .040" thru-holes in these valves. To operate, all ports must be either connected to a line of your system or plugged. Built-in positioning detents allow these valves to snap into place, ensuring the thru-hole is properly aligned.
Standard manual valves (V-100D, V-100L- and V100T) measure 1.80" (45.7 mm) in length. Bulkhead versions (V-101 D, V-101 L and V-101 T) are 2.18" (55.4 mm) long.
 The bulkhead mountable manual configuration can also be mounted on our M-615-1 Valve Bracket (see below). DC gear motor actuated versions are also available.
Selected applications for our Medium Pressure Switching Valves are listed on the following page. However, there are also several other possible uses for these valves.

 

Ventil Halterung VALVE BRACKETS
Mount the bulkhead mountable manual valves presented with these Brackets. Once mounted, a valve will be positioned horizontally. Extra holes are provided for mounting accessories.
Made of sturdy anodized aluminum, these brackets can be attached to any lab surface. Each bracket comes with the required valve mounting hardware and instructions.

 

Artikelnummer Beschreibung Swept Volume Preis in €
MEDIUM PRESSURE 4-PORT SWITCHING VALVES, MANUAL
  V-100D 4-Way Diagonal Flow Switching Valve (1) 12.4 µl 104,44
  V-100L Right Angle Flow Switching Valve(1) 6.2 µl 104,44
  V-100T 3-Way Flow Switching Valve (1) 9.7 µl 104,44
  V-101D Bulkhead Version of V-100D (1) 12.4 µl 110,11
  V-101L Bulkhead Version of V-100L (1) 6.2 µl 110,11
  V-101T Bulkhead Version of V-100T (1) 9.7 µl 110,11
V-103 .050" Allen Wrench (replacement)   2,50
MEDIUM PRESSURE 4-PORT SWITCHING VALVES, ACTUATED
V-1101D-DC Actuated version of V-101D (1),(2) 12.4 µl 1420,37
V-1101L-DC Actuated version ofV-101L (1),(2) 6.2 µl 1420,37
V-1101T-DC Actuated version of V-101T (1),(2) 9.7 µl 1420,37
VALVE BRACKET
Artikelnummer Beschreibung Preis in €
M-615-1 Mounting Bracket for Switching Valves 35,27
M-615-2 Mounting Bracket for Injection and Selection Valves 35,27
(1) Comes complete with P-218BLN/P-240 Flangeless Fittings. L and T valve versions also include a P-309 Plug.
(2) Actuated valves also include: (1) serial port adapter; (1) each RS-232 and contact closure communications cables (1) power adapter, (1) each North American style and European style power cord, DC gear actuated valves come with a communication cable for multiplex (daisy-chain) operations

 

SHUT-OFF  VALVES
-
For Medium Pressure Applications / Biocompatible, All-Polymer Flow Path / Available for 1/16" and 1/8" OD Tubing
Stop a flow stream quickly with Upchurch Scientific® biocompatible Shut-Off Valves. The bodies are manufactured from either PEEK™ or TefzeF® (ETFE) with a Kel-F® rotor, making them highly resistant to chemical attack. The blue colorant used in some valve configurations has proven not to leach out with common HPLC solvents.
Connect semi-rigid or rigid tubing, such as PEEK, stainless steel or Teflon®, with the 1/4-28 Flangeless Fittings provided. Soft tubing, such as Pharmed® or Tygon® , may be connected to these valves using our 1/4-28 barbed adapters.

 

SHUT-OFF VALVES
Artikelnummer Material OD Tubing Thru-hole Volume (1) Pressure Rating Preis in €
P-732 (2) PEEK, natural 1/16" .020" 2.5 µl 500 psi (34 bar) 74,06
P-733 (3) PEEk, natural 1/8" .040" 10.0 µl 500 psi (34 bar) 74,06
P-782 (2) ETFE, blue 1/16" .020" 2.5 µl 500 psi (34 bar) 43,05
P-783 (3) ETFE, blue 1/8" .040" 10.0 µl 500 psi (34 bar) 43,05
P-721 (4) ETFE, natural 1/8" .040" 10.0 µl 500 psi (34 bar) 43,05
(1) Maximum internal volume, with valve fully open (2) Includes P-235 /P-200 Fittings (3) Includes P-335 /P-300 Fitting (4) Includes P-335 /P-300N Fittings

 

Mikro Splitter Ventile MICRO-SPLITTER VALVES
-
For Interfacing LC-MS Systems
/ Split Stream Flow Rates as Low as 2µl/min. / Medium and High Pressure Versions
MICRO-SPLITTER VALVE INFORMATION Upchurch Scientific® offers a line of Micro-Splitter Needle Valves designed to accurately split and control a low-flow stream off a single incoming supply.
The biocompatible Medium Pressure Micro-Splitter Valves are perfect for LC-MS and other multidetector systems, and fraction collectors. The ideal placement of these valves is on the effluent side of the detector flow cell, at a maximum pressure of 800 psi (55 bar). Choose between 1/4-28 and 10-32 threaded versions. A valve is also available to accommodate applications involving capillary tubing.(1)
The High Pressure Micro-Splitter Valves are designed to operate under pressures up to 4,000 psi (276 bar). These products are well suited for running two analytical devices in parallel. The High Pressure Capillary Micro-Splitter Valves (1) may also be used to adapt an analytical HPLC system to handle microbore applications.
Our Graduated Valves offer many of the benefits and features of our original Micro-Splitter Valves, plus the ability to adjust and set the split flow to repeatable settings. This allows documentation of settings and the resulting flow rates for easier method development. The graduations also make it easier to employ the valve in a system used to run multiple analyses that require different split flow rates. Choose from regular High Pressure and Capillary (1) versions.
All Micro-Splitter Valves have been tested at flow rates to 100ml/min., with a maximum resulting pressure drop of only 45 psi (3.1 bar). (2)
(1)
This valve has a MicroTight ` 6-32 threaded fitting on the split stream Select the appropriately sized Micro Tight Tubing Sleeve to connect your capillary tubing.
(2) Preasure drop measured when valves fully opened.
  Valve Typ Threads Internal Volume (1) (closed /fully open) Max. Operating Pressure (psi/bar) Min.Split Flow rate (2)
P-450 Medium Pressure 1/4-28 2.1 / 4.1µl 800 /55 2µL /min
P-451 Medium Pressure 10-32 1.2 / 2.8µl 800 /55 2µL /min
P-452 Medium Pres. Capillary 10-32 /6-32 1.2 / 2.4µl 800 /55 2µL /min
P-460S, T High Pressure 10-32 1.2 / 2.8µl 4,000 /276 4.8µL /min
P-470 High Pres. Graduated 10-32 1.2 / 2.8µl 4,000 /276 4.8µL /min
M-405S,T High Pres. Capillary 10-32 /6-32 1.2 / 2.4µl 4,000 /276 4.8µL /min
M-472 High Pres. Cap. Grad. 10-32 /6-32 1.2 / 2.4µl 4,000 /276 4.8µL /min
(1) The supply and waste port thru-holes have IDs of .0202. The ID for the split-stream port thru-hole is .020" in standart versions; in capillary version it is .010". (2) All tests conducted at an incoming flow rate of 1mL/min. using room temperature water, with equal pressures on both effluent streams. Lower incoming flow rates will result in a gradual loss ofsensitivity when setting the split rate. (2)

 

Artikelnummer Beschreibung Preis in €
MICRO-SPLITTER VALVES
M-405S High Pressure Capillary, 10-32/6-32, with stainless steel needle Includes: (2) F-120 PEEK Fingertight Fittings for 1/16" OD tubing and (1) F-125 PEEK Micro Fingerfight for capillary tubing (1) 123,50
M-405T High Pressure Capillary, 10-32/6-32, with titanium needle
Includes: (2) F-120 PEEK Fingerfight Fittings for 1/16" OD tubing and (1) F-125 PEEK Micro Fingertight for capillary tubing (1)
167,68
P-450 Medium Pressure, 1/4-28, Biocompatible
Includes: (3) P-200 Tefzel® (ETFE) Ferrules and
(3) P-235 PEEK Flangeless Nuts for 1/16" OD tubing
63,96
P-451 Medium Pressure, 10-32, Biocompatible
Includes: (3) F-120 PEEK Fingertight Fittings for 1/16" OD tubing
63,96
P-452 Medium Pressure Capillary, 10-32/6-32, Biocompatible
Includes: (2) F-120 PEEK Fingertight Fittings for 1/16" OD tubing (1) F-125 PEEK Micro Fingertight for capillary tubing (1)
63,96
P-460S High Pressure, 10-32, with stainless steel needle Includes: (3) F-120 PEEK Fingertight Fittings for 1/16" OD tubing 116,18
P-460T High Pressure, 10-32, with titanium needle
Includes: (3) F-120 PEEK Fingertight Fittings for 1/16" OD tubing
167,68
GRADUATED MICRO-SPLITTER VALVES
P-470 High Pressure Graduated, 10-32, with stainless steel needle Includes: (3) F-120 PEEK Fingertight Fittings for 1/16" OD tubing 348,66
M-472 High Pressure Capillary Graduated, 10-32/6-32, with stainless steel needle Includes: (2) F-120 PEEK Fingertight Fittings for 1/16" OD tubing and (1) F-125 PEEK Micro Fingertight for capillary tubing (1) 361,94
(1) Use with our MicroTight Tubing Sleeves

 

MICRO-METERING VALVES
- Flow Rates as Low as 3.5ul/min (1) / 1/4-28 and 10-32 Designs Available / PEEK™ Polymer Construction, with Teflon® Seals
(1) At 1.0 ml/min incoming flow rate with room temperature water.
For fine control of fluid flow rates, our Micro-Metering Needle Valves can reduce outgoing flow to as low as 3.5 µL/min (1). These needle valves are perfect for use with peristaltic pump fluid-transfer applications, mass spectrometry, and fraction collection.
Upchurch Scientific® Micro-Metering Valves can also be used to regulate gas flow in helium sparging lines and as a flow-dependent variable back pressure regulator.
Flow path materials are PEEK polymer and Teflon (O-rings). All versions of this valve have .020" thru-holes.

 

MICRO-METERING VALVES
Artikelnummer Material OD Tubing Thru-hole Internal Volume (1) Pressure Rating Preis in €
P-445 (2) PEEK, black 1/16" .020" 7.7 µl 800 psi (55 bar) 50,88
P-446 (3) PEEK, black 1/16" .020" 7.2 µl 800 psi (55 bar) 58,09
P-447 (4) PEEK, black 1/8" .020" 7.7 µl 800 psi (55 bar) 50,88
(1) Maximum internal volume, with valve fully open. (2) Includes 1/4-28 P-230 P-200 Flangeless fittings. (3) Includes 10-32 F-120 One-Piece Fingertight Fittings. (4) Includes 1/4-28 P-330 /P-300 Flangeless Fittings.

 

PRIME/PURGE VALVE FOR WATER® PUMPS
- Automatic Valve Operation with a Simple Twist of a Luer Lock Syringe /
No Tubing to Cut or Ferrules to Swage
/ No Wear on the Internal Seal
UNIVERSAL PRIME/PURGE VALVES
For Any Style HPLC System / Automatic Luer Syringe Operation / Featuring Handy Mounting Holes
The Upchurch Scientific® Prime/Purge Valve for Waters pumps automatically opens when a luer syringe is attached and closes when the syringe is removed. No valve rotation is required after the initial installation, so wear on the internal seal is eliminated.
In addition, our Waters-compatible Prime/Purge Valve is simpler to operate and more economically priced than alternative valves available for Waters systems. This valve is constructed of rugged materials, including a PEEK™ valve body. The component structure ensures compatibility with virtually all common solvents used in HPLC analyses. A Waters-compatible internal Teflon® seal is included with the valve. This seal can also be purchased separately. It can be used both with the Upchurch Scientific valve and the original valve supplied with the pump.

Purge Ventile

Upchurch Scientific Universal Prime/Purge Valves are easy to operate. Simply install a valve along the flow path with the included fittings and attach
a luer-tipped syringe. Then, withdraw the plunger and watch as solvent and residual bubbles are removed from the solvent line. The valves automatically close when the syringe is removed.
The low pressure version of the valve is designed to be used with 1/8" OD tubing, while the high pressure version accommodates 1/16" OD tubing. Optional mounting is made easy by the handy holes in the body of each unit.
Air in the Pumphead
Air within the pumphead can cause flow instability and noisy pump operation. Place the High Pressure Prime/Purge Valve between the pump and the sample injector, where it can be used to remove bubbles that have become lodged within your pump. This valve is rated for a maximum pressure of 5,000 psi (345 bar).
Air in the Inlet Solvent Line
Install the Low Pressure Universal Prime/Purge Valve along the inlet solvent path near the pump to remove bubbles from the inlet solvent line. The valve can also be used to rapidly "wet" your solvent inlet filter. When a new filter is installed, it often contains a substantial amount of air within its pores. At standard flow rates, it may require several minutes before the inlet fluid pathway is completely free of gas. Using this valve, you are able to rapidly draw solvent through the inlet filter, dislodging the gas and minimizing downtime.

 

PRIME /PURGE VALVES
Artikelnummer Beschreibung Preis in €
V-320 Prime/Purge Valve for Waters Pumps Includes (1) V-320-06 Teflon seal 179,84
V-320-06 Replacement Teflon Seal (for V-320) 6,90
V-321  Low Pressure Universal Prime/Purge Valve Includes (2) P-300N Tefzell Ferrules & (2) P-335 PEEK Nuts, for 1/8" OD tubing 179,84
V-322 High Pressure Universal Prime/Purge Valve Includes (2) F-120 Fittings for 1/16" OD tubing 179,84
B-310 10cc Disposable Luer-Tipped Syringe 0,93